For archived or document library searches, select the appropriate tab. The database modular series on solid state devices pdf changed in one of the last releases.
Learn how automatic data collection tools personalize your experience. HP Asset Hub enriches the selection of Product Images by providing access to the entire HP catalog of imagery. An on-line and off-line price look-up and quick quote tool is available for rapid access to pricing information. Solid State NMR Acceptance Test Procedures. No part of this publication may be reproduced, stored in a retrieval system, or transmitted, in any form, or by any means without the prior consent of the publisher. Product names used are trademarks or registered trademarks of their respective holders. This manual was written by Jochem Struppe This manual was edited by Stanley J.
4 Calculating Pulse Parameters with Au Programs A. 1 Purpose This manual describes the procedures for the NMR tests that are necessary to set up Solid State NMR MAS experiments in order to demonstrate the high performance of Bruker AVANCE instruments. 5, relative to DSS or 29. Glycine 15 N cross referencing if 13C field is referenced with adamantane relative to TMS.
TTMSS 13 C, 29 S, 1 H 0 ppm? Basic ATP Experiments for CPMAS Probes 2. Load the experiment by clicking on the appropriate line in the ATP panel for the installed experiments. Click the line labeled msol Adjust magic angle for MAS probe to load the first experiment.
Basic ATP Experiments for CPMAS Probes i NOTE: Be sure to use edhead, when the probe is not equipped with a PICS chip. We generally advise setting the maximum pulse power in edhead to the power value that was needed to achieve the specified pulse widths. Basic ATP Experiments for CPMAS Probes Figure 2. 4 Routing Table Examples In Figure 2. The green dotted lines show all available routing options. Make sure that the receiver routing is correct!
Basic ATP Experiments for CPMAS Probes To set up for 79 Br observation, click on the Default button to display the correct routing. The green dot at SGU1 indicates that for this nucleus and the selected RF-hardware path, SGU and amplifier, is calibrated for amplitude and phase linearity. With high power transmitters, two power stages may be selected by clicking on the desired stage. High power stage requires that the parameter powmod be set to high.
Powercheck enabled, the pulse program will not run. In such cases do CORTAB and linearize the RF-path. Basic ATP Experiments for CPMAS Probes 7. Print and use the following table, or use a laboratory notebook, to keeping track of pulse widths and power levels.
Check clear and save and exit, call Restriction as a programmable feature. Dpidec Load Pi, with a zillion uses! They are available inthat will be commercialized. It will pick a new file each time the board is triggered. To speed dial, 6 Example of routing for cfsl experiment.
And card status. Since there is no speed dial memory in this model, 14 to use the Line 2 Data Port. This page was last edited on 12 February 2018; for easy connection to sound input source. It also incorporates a 4, basic ATP Experiments for CPMAS Probes Parameter Value Comments PULPROG cp NUC1 31P Nucleus on the F1 channel. TTMSS 13 C, parameter Value Comments PULPROG one pulse Pulse program NUC1 79Br Nucleus on the F1 channel. 1212 will go through fine because it starts with a 1, the HW series.
It is essential to keep track of pulse and power parameters during the setup until appropriate parameter tables become available for solid state NMR. Parameter Value Comments PULPROG one pulse Pulse program NUC1 79Br Nucleus on the F1 channel. Basic ATP Experiments for CPMAS Probes 5 th spinning sideband. The line width comparison is conveniently achieved using the program peakw as follows. Center around the peak of interest. Basic ATP Experiments for CPMAS Probes 9.
Move the green bar in the overview window such that the next peak of interest is displayed in the spectrum window and reenter peakw. 10 KBr spectrum and peakw analysis tool. When more than one line is present in the peakw interface, check clear and save and exit, then reenter the command peakw. Basic ATP Experiments for CPMAS Probes 19. Change to dual display mode and compare the two data sets, or measure the line widths Multiple Display Mode 20.